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Unit of study_

MECH5311: Microscopy and Microanalysis of Materials

This UoS offers the fundamental knowledge that is essential for the microscopy and microanalysis of materials. The UoS will cover the basic fundamental concepts of materials structures and modern materials characterisation techniques that are available in Sydney Microscopy and Microanalysis in the University, including X-ray diffraction, scanning electron microscopy, transmission electron microscopy, and atom probe tomography.

Details

Academic unit Aerospace, Mechanical and Mechatronic
Unit code MECH5311
Unit name Microscopy and Microanalysis of Materials
Session, year
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Semester 1, 2022
Attendance mode Normal day
Location Remote
Credit points 6

Enrolment rules

Prohibitions
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None
Prerequisites
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None
Corequisites
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None
Assumed knowledge
? 

AMME1362 or AMME2302 or AMME9302 or CIVL2110

Available to study abroad and exchange students

Yes

Teaching staff and contact details

Coordinator Xiaozhou Liao, xiaozhou.liao@sydney.edu.au
Type Description Weight Due Length
Assignment Assignment 3
Students will works on questions based on the lectures in weeks 10 -- 13.
20% STUVAC
Due date: 03 Jun 2021
N/A
Outcomes assessed: LO1 LO2 LO3 LO4 LO6 LO9
Assignment Assignment 1
Students will works on questions based on the lectures in weeks 1 -- 4.
20% Week 06
Due date: 01 Apr 2021
N/A
Outcomes assessed: LO1 LO2 LO3 LO4 LO5
Assignment Assignment 2
Students will works on questions based on the lectures in weeks 6 -- 9.
20% Week 10
Due date: 06 May 2022
N/A
Outcomes assessed: LO1 LO2 LO3 LO4 LO6 LO7 LO8
Presentation group assignment Presentation
Group presentations on materials characterisation using advanced microscopy
20% Week 11
Due date: 13 May 2022
20 min presentation + 5 min Q&A
Outcomes assessed: LO1 LO2 LO3 LO4 LO5 LO6 LO7 LO8 LO9
Assignment group assignment presentation written report
Essay. A group written report based on students' oral presentation.
20% Week 13
Due date: 27 May 2022
~3,000 words
Outcomes assessed: LO1 LO2 LO3 LO4 LO5 LO6 LO7 LO8 LO9
group assignment = group assignment ?

Seminar and report, and three assignments

Assessment criteria

Detailed information for each assessment can be found on Canvas.

Late submission

In accordance with University policy, these penalties apply when written work is submitted after 11:59pm on the due date:

  • Deduction of 5% of the maximum mark for each calendar day after the due date.
  • After ten calendar days late, a mark of zero will be awarded.

This unit has an exception to the standard University policy or supplementary information has been provided by the unit coordinator. This information is displayed below:

In accordance with University policy, these penalties apply when written work is submitted after 11:59 pm on the due date: • Deduction of 5% of the maximum mark for each calendar day after the due date. • After ten calendar days late, a mark of zero will be awarded.

Special consideration

If you experience short-term circumstances beyond your control, such as illness, injury or misadventure or if you have essential commitments which impact your preparation or performance in an assessment, you may be eligible for special consideration or special arrangements.

Academic integrity

The Current Student website provides information on academic honesty, academic dishonesty, and the resources available to all students.

The University expects students and staff to act ethically and honestly and will treat all allegations of academic dishonesty or plagiarism seriously.

We use similarity detection software to detect potential instances of plagiarism or other forms of academic dishonesty. If such matches indicate evidence of plagiarism or other forms of dishonesty, your teacher is required to report your work for further investigation.

WK Topic Learning activity Learning outcomes
Ongoing Independent study Independent study (110 hr) LO1 LO2 LO3 LO4 LO5 LO6 LO7 LO8 LO9
Week 01 Brief review of structures and defects in crystalline materials Lecture (3 hr) LO1
Week 02 Reciprocal space Lecture (3 hr) LO2
Week 03 X-ray diffraction and electron–matter interactions Lecture (3 hr) LO4 LO5
Week 04 Atom probe tomography Lecture (3 hr) LO3
Week 06 Sample preparation for APT, SEM & TEM Lecture (3 hr) LO6
Week 07 Scanning electron microscopy -- the Instrument, back-scattered imaging, secondary electron imaging Lecture (3 hr) LO3 LO4 LO7
Week 08 Scanning electron microscopy -- Electron backscattered diffraction; Transmission electron microscopy -- the Instrument Lecture (3 hr) LO3 LO4 LO8 LO9
Week 09 Transmission electron microscopy -- Diffraction, imaging Lecture (3 hr) LO3 LO4 LO9
Week 10 Transmission electron microscopy -- imaging Lecture (3 hr) LO3 LO4 LO9
Week 11 Seminar presentation Lecture (3 hr) LO1 LO2 LO3 LO4 LO5 LO6 LO7 LO8 LO9
Week 12 Spectroscopy and in-situ microscopy Lecture (3 hr) LO3 LO4 LO7 LO8 LO9
Week 13 In-situ microscopy and lab tour Lecture (3 hr) LO3 LO4 LO6 LO7 LO8 LO9

Study commitment

Typically, there is a minimum expectation of 1.5-2 hours of student effort per week per credit point for units of study offered over a full semester. For a 6 credit point unit, this equates to roughly 120-150 hours of student effort in total.

Required readings

  1. Materials Science and Engineering: An Introduction, 10th edition, William D. Callister, Jr. and David G. Rethwisch, Wiley, ISBN 9781119405498
     
  2. Scanning Electron Microscopy and X-Ray Microanalysis, 3rd edition, Joseph Goldstein, et al., Springer Science+Business Media, LLC, ISBN 978-1-4615-0215-9 (eBook)
     
  3. Transmission Electron Microscopy, C. Barry Carter and David B. Williams, Spring, ISBN 978-3-319-26651-0 (eBook)
     
  4. Scanning Transmission Electron Microscopy, Stephen J. Pennycook and Peter D. Nellist, Spring, ISBN 978-1-4419-7200-2 (eBook)
     
  5. Atom Probe Microscopy, Baptiste Gault, Michael P. Moody, Julie M. Cairney, and Simon P. Ringer, Spring, ISBN 978-1-4614-3436-8 (eBook)
     

Learning outcomes are what students know, understand and are able to do on completion of a unit of study. They are aligned with the University’s graduate qualities and are assessed as part of the curriculum.

At the completion of this unit, you should be able to:

  • LO1. communicate effectively the microstructures, crystalline structures and crystalline defects of materials in oral and/or written presentations
  • LO2. describe, in relatively simple terms, crystalline lattice structures in reciprocal space, describing theoretically, schematically, and mathematically
  • LO3. communicate effectively several common microstructural characterisation techniques in oral and/or written presentations
  • LO4. describe, in relatively simple terms, the interactions of fast electrons with matter, describing theoretically, schematically, and mathematically
  • LO5. identify crystalline phases using X-ray diffraction and determine crystalline lattice structures using electron diffraction
  • LO6. understand common materials preparation techniques for structural characterisation
  • LO7. understand the basic working mechanism of the scanning electron microscope and microstructural information that can be extracted from electron backscattered images and secondary electron images
  • LO8. understand the basic working mechanism of electron backscatter diffraction and its applications in structural characterisation of materials
  • LO9. understand the basic working mechanisms of the transmission electron microscope, including electron diffraction, imaging and spectrometry, and their applications in materials characterisation

Graduate qualities

The graduate qualities are the qualities and skills that all University of Sydney graduates must demonstrate on successful completion of an award course. As a future Sydney graduate, the set of qualities have been designed to equip you for the contemporary world.

GQ1 Depth of disciplinary expertise

Deep disciplinary expertise is the ability to integrate and rigorously apply knowledge, understanding and skills of a recognised discipline defined by scholarly activity, as well as familiarity with evolving practice of the discipline.

GQ2 Critical thinking and problem solving

Critical thinking and problem solving are the questioning of ideas, evidence and assumptions in order to propose and evaluate hypotheses or alternative arguments before formulating a conclusion or a solution to an identified problem.

GQ3 Oral and written communication

Effective communication, in both oral and written form, is the clear exchange of meaning in a manner that is appropriate to audience and context.

GQ4 Information and digital literacy

Information and digital literacy is the ability to locate, interpret, evaluate, manage, adapt, integrate, create and convey information using appropriate resources, tools and strategies.

GQ5 Inventiveness

Generating novel ideas and solutions.

GQ6 Cultural competence

Cultural Competence is the ability to actively, ethically, respectfully, and successfully engage across and between cultures. In the Australian context, this includes and celebrates Aboriginal and Torres Strait Islander cultures, knowledge systems, and a mature understanding of contemporary issues.

GQ7 Interdisciplinary effectiveness

Interdisciplinary effectiveness is the integration and synthesis of multiple viewpoints and practices, working effectively across disciplinary boundaries.

GQ8 Integrated professional, ethical, and personal identity

An integrated professional, ethical and personal identity is understanding the interaction between one’s personal and professional selves in an ethical context.

GQ9 Influence

Engaging others in a process, idea or vision.

Outcome map

Learning outcomes Graduate qualities
GQ1 GQ2 GQ3 GQ4 GQ5 GQ6 GQ7 GQ8 GQ9
No changes have been made since this unit was last offered.

Site visit guidelines

We may arrange a lab tour to the Australian Center for Microscopy and Microanalysis in Madsen Building if the COVID restrictions are lifted.

Disclaimer

The University reserves the right to amend units of study or no longer offer certain units, including where there are low enrolment numbers.

To help you understand common terms that we use at the University, we offer an online glossary.